Abstract
High-speed synchrotron tomography was used to investigate the nucleation and growth dynamics of Al13Fe4 intermetallic during solidification of an Al-5wt%Fe alloy, providing new insights into its formation process. The majority of Al13Fe4 intermetallics nucleated near the surface oxide of the specimen and a few nucleated at Al13Fe4 phase. Al13Fe4 crystals grew into a variety of shapes, including plate-like, hexagonal tabular, stair-like and V-shaped, which can be attributed to the crystal structure of this compound and its susceptibility to twinning. Hole-like defects filled with aluminium melt were observed within the intermetallics. Orentied particle attachement mechanism was proposed to explain the formation of the Al13Fe4 intermetialic, which needs further experiments and simulation to confirm.
Original language | English |
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Article number | 158604 |
Journal | Journal of Alloys and Compounds |
Volume | 861 |
Early online date | 5 Jan 2021 |
DOIs | |
Publication status | E-pub ahead of print - 5 Jan 2021 |
Bibliographical note
Not yet published 08/01/2021Keywords
- 4D imaging
- Al alloy
- Faceted crystal
- Synchrotron tomography
ASJC Scopus subject areas
- Mechanics of Materials
- Mechanical Engineering
- Metals and Alloys
- Materials Chemistry
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